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1

Detection, identification and quantification by 1H NMR of adulterants in 150 herbal dietary supplements marketed for improving sexual performance

Gilard, Véronique, Balayssac, Stéphane, Tinaugus, Aurélie, Martins, Nathalie, Martino, Robert, Malet-Martino, Myriam

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2015

Language:

english

File:

PDF, 2.27 MB

english, 2015

2

Counterfeit drugs: analytical techniques for their identification

R. Martino, M. Malet-Martino, V. Gilard, S. Balayssac

Journal:

Analytical and Bioanalytical Chemistry

Year:

2010

Language:

english

File:

PDF, 1.16 MB

english, 2010

3

Identification of a novel sildenafil analogue in an adulterated herbal supplement

Julie Vaysse, Véronique Gilard, Stéphane Balayssac, Chantal Zedde, Robert Martino, Myriam Malet-Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2012

Language:

english

File:

PDF, 1.06 MB

english, 2012

4

Analysis of adulterated herbal medicines and dietary supplements marketed for weight loss by DOSY 1H-NMR

Vaysse, J., Balayssac, S., Gilard, V., Desoubdzanne, D., Malet-Martino, M., Martino, R.

Journal:

Food Additives & Contaminants Part A

Year:

2010

Language:

english

File:

PDF, 840 KB

english, 2010

5

Evaluation of a Benchtop Cryogen-Free Low-Field 1 H NMR Spectrometer for the Analysis of Sexual Enhancement and Weight Loss Dietary Supplements Adulterated with Pharmaceutical Substances

Pagès, Guilhem, Gerdova, Anna, Williamson, David, Gilard, Véronique, Martino, Robert, Malet-Martino, Myriam

Journal:

Analytical Chemistry

Year:

2014

Language:

english

File:

PDF, 1.90 MB

english, 2014

6

Proton NMR for detection, identification and quantification of adulterants in 160 herbal food supplements marketed for weight loss

Hachem, Rabab, Assemat, Gaëtan, Martins, Nathalie, Balayssac, Stéphane, Gilard, Véronique, Martino, Robert, Malet-Martino, Myriam

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2016

Language:

english

File:

PDF, 1.53 MB

english, 2016

7

A review of synthetic phosphodiesterase type 5 inhibitors (PDE-5i) found as adulterants in dietary supplements

Kee, Chee-Leong, Ge, Xiaowei, Gilard, Véronique, Malet-Martino, Myriam, Low, Min-Yong

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2017

Language:

english

File:

PDF, 1.64 MB

english, 2017

8

The usefulness of 2D DOSY and 3D DOSY-COSY 1H NMR for mixture analysis: application to genuine and fake formulations of sildenafil (Viagra)

Saleh Trefi, Véronique Gilard, Stéphane Balayssac, Myriam Malet-Martino, Robert Martino

Journal:

Magnetic Resonance in Chemistry

Year:

2009

Language:

english

File:

PDF, 604 KB

english, 2009

9

2D and 3D DOSY 1H NMR, a useful tool for analysis of complex mixtures: Application to herbal drugs or dietary supplements for erectile dysfunction

Stéphane Balayssac, Saleh Trefi, Véronique Gilard, Myriam Malet-Martino, Robert Martino, Marc-André Delsuc

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2009

Language:

english

File:

PDF, 1.13 MB

english, 2009

10

Generic ciprofloxacin tablets contain the stated amount of drug and different impurity profiles: A 19F, 1H and DOSY NMR analysis

Saleh Trefi, Véronique Gilard, Myriam Malet-Martino, Robert Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2007

Language:

english

File:

PDF, 689 KB

english, 2007

11

Analysis of illegally manufactured formulations of tadalafil (Cialis®) by 1H NMR, 2D DOSY 1H NMR and Raman spectroscopy

Saleh Trefi, Corinne Routaboul, Saleh Hamieh, Véronique Gilard, Myriam Malet-Martino, Robert Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2008

Language:

english

File:

PDF, 796 KB

english, 2008

12

Quality Assessment of Commercial Magnoliae Officinalis Cortex by 1H-NMR-based Metabolomics and HPLC Methods

Yong Jiang, Julie Vaysse, Véronique Gilard, Stéphane Balayssac, Sébastien Déjean, Myriam Malet-Martino, Bruno David, Christel Fiorini, Yves Barbin

Journal:

Phytochemical Analysis

Year:

2012

Language:

english

File:

PDF, 1.88 MB

english, 2012

13

Analysis of herbal dietary supplements for sexual performance enhancement: First characterization of propoxyphenyl-thiohydroxyhomosildenafil and identification of sildenafil, thiosildenafil, phentolamine and tetrahydropalmatine as adulterants

Stéphane Balayssac, Véronique Gilard, Chantal Zedde, Robert Martino, Myriam Malet-Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2012

Language:

english

File:

PDF, 1.02 MB

english, 2012

14

First identification and quantification of lorcaserin in an herbal slimming dietary supplement

Hachem, Rabab, Malet-Martino, Myriam, Gilard, Véronique

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2014

Language:

english

File:

PDF, 632 KB

english, 2014

15

Screening of “Spice” herbal mixtures: From high-field to low-field proton NMR

Assemat, Gaëtan, Dubocq, Florian, Balayssac, Stéphane, Lamoureux, Catherine, Malet-Martino, Myriam, Gilard, Véronique

Journal:

Forensic Science International

Year:

2017

Language:

english

File:

PDF, 853 KB

english, 2017

16

Pulsed-field gradient nuclear magnetic resonance measurements (PFG NMR) for diffusion ordered spectroscopy (DOSY) mapping

Pagès, Guilhem, Gilard, Véronique, Martino, Robert, Malet-Martino, Myriam

Journal:

The Analyst (Royal Society of Chemistry)

Year:

2017

Language:

english

File:

PDF, 2.55 MB

english, 2017

17

Diffusion-ordered spectroscopy on a benchtop spectrometer for drug analysis

Assemat, Gaëtan, Gouilleux, Boris, Bouillaud, Dylan, Farjon, Jonathan, Gilard, Véronique, Giraudeau, Patrick, Malet-Martino, Myriam

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2018

Language:

english

File:

PDF, 1.71 MB

english, 2018

18

ChemInform Abstract: The Analysis of Cyclophosphamide and Its Metabolites

Myriam Malet-Martino, Veronique Gilard, Robert Martino

Journal:

Year:

1999

File:

PDF, 24 KB

1999

19

ChemInform Abstract: A New Method for the Synthesis of 5-Fluorouracil Prodrugs.

Pascale Jolimaitre, Christiane Andre-Barres, Myriam Malet-Martino, Robert Martino, Isabelle Rico-Lattes

Journal:

Year:

2000

File:

PDF, 26 KB

2000

20

Direct 19f NMR spectroscopic observation of 5-fluorouracil metabolism in the isolated perfused mouse liver model

S. Cabanac, M. C. Malet-Martino, M. Bon, R. Martino, J. F. Nedelec, J. L. Dimicoli

Journal:

NMR in Biomedicine

Year:

1988

Language:

english

File:

PDF, 775 KB

english, 1988

21

Efficient approach to acyloxymethyl esters of nalidixic acid and in vitro evaluation as intra-ocular prodrugs

Joëlle Azéma, Brigitte Guidetti, Myriam Malet-Martino, Robert Martino, Christine Roques

Journal:

Bioorganic & Medicinal Chemistry

Year:

2006

Language:

english

File:

PDF, 358 KB

english, 2006

22

Interaction mechanisms between caffeine and polyphenols in infusions of Camellia sinensis leaves

Aurélie Couzinet-Mossion, Stéphane Balayssac, Véronique Gilard, Myriam Malet-Martino, Martine Potin-Gautier, Philippe Behra

Journal:

Year:

2010

Language:

english

File:

PDF, 703 KB

english, 2010

23

Application of fluorine-19 nuclear magnetic resonance to the determination of plasma-protein binding of 5′-deoxy-5-fluorouridine, a new antineoplastic fluoropyrimidine

D. Meynial, A. Lopez, M.C. Malet-Martino, J.S. Hoffmann, R. Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

1988

Language:

english

File:

PDF, 884 KB

english, 1988

24

7-((4-Substituted)piperazin-1-yl) derivatives of ciprofloxacin: Synthesis and in vitro biological evaluation as potential antitumor agents

Joëlle Azéma, Brigitte Guidetti, Janique Dewelle, Benjamin Le Calve, Tatjana Mijatovic, Alexander Korolyov, Julie Vaysse, Myriam Malet-Martino, Robert Martino, Robert Kiss

Journal:

Bioorganic & Medicinal Chemistry

Year:

2009

Language:

english

File:

PDF, 676 KB

english, 2009

25

Novel lipophilic 7H-pyrido[1,2,3-de]-1,4-benzoxazine-6-carboxylic acid derivatives as potential antitumor agents: Improved synthesis and in vitro evaluation

Alexander Korolyov, Sandra Dorbes, Joëlle Azéma, Brigitte Guidetti, Mathieu Danel, Delphine Lamoral-Theys, Thierry Gras, Jacques Dubois, Robert Kiss, Robert Martino, Myriam Malet-Martino

Journal:

Bioorganic & Medicinal Chemistry

Year:

2010

Language:

english

File:

PDF, 474 KB

english, 2010

26

Étude critique de l'utilisation de la RMN HR-MAS pour l'analyse des tissus biologiques

Franck Desmoulin, Delphine Bon, Robert Martino, Myriam Malet-Martino

Journal:

Comptes Rendus Chimie

Year:

2008

File:

PDF, 712 KB

2008

27

Fluorine-19 or phosphorus-31 NMR spectroscopy: A suitable analytical technique for quantitative in vitro metabolic studies of fluorinated or phosphorylated drugs

Robert Martino, Véronique Gilard, Franck Desmoulin, Myriam Malet-Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2005

Language:

english

File:

PDF, 660 KB

english, 2005

28

Simultaneous assay of organic fluorine compounds in biological fluids by fluorine-19 nuclear magnetic resonance spectrometry over a large spectral width: Application to Fluoropyrimidines

J.P. Beteille, A. Lopez, M. Bon, M.C. Malet-Martino, R. Martino

Journal:

Analytica Chimica Acta

Year:

1985

Language:

english

File:

PDF, 458 KB

english, 1985

29

Fluorouracil prodrugs for the treatment of proliferative vitreoretinopathy: formulation in silicone oil and in vitro release of fluorouracil

Pascale Jolimaı̂tre, Myriam Malet-Martino, Robert Martino

Journal:

International Journal of Pharmaceutics

Year:

2003

Language:

english

File:

PDF, 179 KB

english, 2003

30

Identification of new aqueous chemical degradation products of isophosphoramide mustard

Stéphane Breil, Robert Martino, Véronique Gilard, Myriam Malet-Martino, Ulf Niemeyer

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2001

Language:

english

File:

PDF, 185 KB

english, 2001

31

Isolation of an unknown metabolite of capecitabine, an oral 5-fluorouracil prodrug, and its identification by nuclear magnetic resonance and liquid chromatography–tandem mass spectrometry as a glucuroconjugate of 5′-deoxy-5-fluorocytidine, namely 2′-(β-d-glucuronic acid)–5′-deoxy-5-fluorocytidine

Franck Desmoulin, Véronique Gilard, Robert Martino, Myriam Malet-Martino

Journal:

Journal of Chromatography B

Year:

2003

Language:

english

File:

PDF, 370 KB

english, 2003

32

Measurement of total water and bound water contents in human stratum corneum by in vitro proton nuclear magnetic resonance spectroscopy

V. GILARD, R. MARTINO, M. MALET-MARTINO, M. RIVIERE, A. GOURNAY, R. NAVARRO

Journal:

International Journal of Cosmetic Science

Year:

1998

Language:

english

File:

PDF, 134 KB

english, 1998

33

Human urinary excretion of doxifluridine and metabolites during a 5-day chemotherapeutic schedule using fluorine-19 nuclear magnetic resonance spectrometry

M. C. Malet-Martino, P. Servin, J. Bernadou, J. P. Armand, R. Martino

Journal:

Investigational New Drugs

Year:

1987

Language:

english

File:

PDF, 443 KB

english, 1987

34

Noninvasive fluorine-19 NMR study of fluoropyrimidine metabolism in cell cultures of human pancreatic and colon adenocarcinoma

Marie-C. Malet-Martino, Françoise Faure, Jean-Pierre Vialaneix, Claude Palevody, Etienne Hollande, Robert Martino

Journal:

Cancer Chemotherapy and Pharmacology

Year:

1986

Language:

english

File:

PDF, 637 KB

english, 1986

35

New approach to metabolism of 5′-deoxy-5-fluorouridine in humans with fluorine-19 NMR

Marie-Catherine Malet-Martino, Robert Martino, André Lopez, Jean-Pierre Béteille, Maryse Bon, Jean Bernadou, Jean-Pierre Armand

Journal:

Cancer Chemotherapy and Pharmacology

Year:

1984

Language:

english

File:

PDF, 466 KB

english, 1984

36

Determination of the urinary excretion of ifosfamide and its phosphorated metabolites by phosphorus-31 nuclear magnetic resonance spectroscopy

V. Gilard, M. C. Malet-Martino, M. Forni, U. Niemeyer, J. C. Ader, R. Martino

Journal:

Cancer Chemotherapy and Pharmacology

Year:

1993

Language:

english

File:

PDF, 777 KB

english, 1993

37

Reduction of the antineoplastic fluoropoyrimidine, 5-fluorouracil, to 5,6-dihydro-5-fluorouracil inEscherichia coli

J. P. Vialaneix, A. Benjamin, M. C. Malet-Martino, R. Martino, G. Michel

Journal:

Biotechnology Letters

Year:

1987

Language:

english

File:

PDF, 308 KB

english, 1987

38

Flucytosine conversion to fluorouracil in humans: Does a correlation with gut flora status exist? A report of two cases using fluorine-19 magnetic resonance spectroscopy

Marie-Catherine Malet-Martino, R. Martino, M. de Forni, A. Andremont, O. Hartmann, J. P. Armand

Journal:

Year:

1991

Language:

english

File:

PDF, 403 KB

english, 1991

39

Analysis of hydrophilic and lipophilic choline compounds in radioresistant and radiosensitive glioblastoma cell lines by HILIC-ESI-MS/MS

D. Desoubzdanne, C. Claparols, N. Martins-Froment, C. Zedde, S. Balayssac, V. Gilard, F. Tercé, R. Martino, M. Malet-Martino

Journal:

Analytical and Bioanalytical Chemistry

Year:

2010

Language:

english

File:

PDF, 416 KB

english, 2010

40

pH optimization for a reliable quantification of brain tumor cell and tissue extracts with1H NMR: focus on choline-containing compounds and taurine

O. Robert, J. Sabatier, D. Desoubzdanne, J. Lalande, S. Balayssac, V. Gilard, R. Martino, M. Malet-Martino

Journal:

Analytical and Bioanalytical Chemistry

Year:

2011

Language:

english

File:

PDF, 10.57 MB

english, 2011

41

Stability of commercial solutions of 5-fluorouracil for continuous infusion in an ambulatory pump

Alexandra Fournet, Véronique Gilard, Myriam Malet-Martino, Robert Martino, Pierre Canal, Marcel De Forni

Journal:

Cancer Chemotherapy and Pharmacology

Year:

2000

Language:

english

File:

PDF, 111 KB

english, 2000

42

Urinary stability of carboxycyclophosphamide and carboxyifosfamide, two major metabolites of the anticancer drugs cyclophosphamide and ifosfamide

Claire Joqueviel, Véronique Gilard, Robert Martino, Myriam Malet-Martino, Ulf Niemeyer

Journal:

Cancer Chemotherapy and Pharmacology

Year:

1997

Language:

english

File:

PDF, 203 KB

english, 1997

43

In vivo31P and1H HR-MAS NMR spectroscopy analysis of the unstarvedAporrectodea caliginosa(Lumbricidae)

Delphine Bon, Véronique Gilard, Stéphane Massou, Guénola Pérès, Myriam Malet-Martino, Robert Martino, Franck Desmoulin

Journal:

Biology and Fertility of Soils

Year:

2006

Language:

english

File:

PDF, 344 KB

english, 2006

44

Dichlorvos degradation studied by31P-NMR

F. Benoit-Marquié, C. de Montety, V. Gilard, R. Martino, M. T. Maurette, M. Malet-Martino

Journal:

Environmental Chemistry Letters

Year:

2004

Language:

english

File:

PDF, 159 KB

english, 2004

45

Two-dimensional DOSY experiment with Excitation Sculpting water suppression for the analysis of natural and biological media

Stéphane Balayssac, Marc-André Delsuc, Véronique Gilard, Yann Prigent, Myriam Malet-Martino

Journal:

Journal of Magnetic Resonance

Year:

2009

Language:

english

File:

PDF, 665 KB

english, 2009

46

Quality assessment of fluoxetine and fluvoxamine pharmaceutical formulations purchased in different countries or via the Internet by 19F and 2D DOSY 1H NMR

Saleh Trefi, Véronique Gilard, Stéphane Balayssac, Myriam Malet-Martino, Robert Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2008

Language:

english

File:

PDF, 809 KB

english, 2008

47

Analytical challenges in drug counterfeiting and falsification—The NMR approach

Ulrike Holzgrabe, Myriam Malet-Martino

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2011

Language:

english

File:

PDF, 909 KB

english, 2011

48

NMR techniques in biomedical and pharmaceutical analysis

M. Malet-Martino, U. Holzgrabe

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2011

Language:

english

File:

PDF, 754 KB

english, 2011

49

Cardiotoxicity of commercial 5-fluorouracil vials stems from the alkaline hydrolysis of this drug

Lemaire, L, Malet-Martino, MC, de Forni, M, Martino, R, Lasserre, B

Journal:

British Journal of Cancer

Year:

1992

Language:

english

File:

PDF, 1.70 MB

english, 1992

50

The anti-cancer drug 5-fluorouracil is metabolized by the isolated perfused rat liver and in rats into highly toxic fluoroacetate

Arellano, M, Malet-Martino, M, Martino, R, Gires, P

Journal:

British Journal of Cancer

Year:

1998

Language:

english

File:

PDF, 1.57 MB

english, 1998

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